A
recent breakthrough in atomic-level analysis will help researchers in
the development of advanced semiconductors and other nanometer-scale
devices and materials. Scientists at FEI's nanotechnology center in
Eindhoven, The Netherlands, broke the 1-Å image-resolution barrier
using a 200-kV transmission electron microscope (see accompanying photos).
This is the first time that images with <1 Å resolution can
be directly viewed using commercially available technologies, according
to the Hillsboro, OR–based metrology company.
The
artifact-free imaging was accomplished with a Tecnai F20 ST TEM that
was equipped with advanced electron optics capabilities
developed by FEI and its partner, Corrected Electron Optical Systems
(CEOS) of Heidelberg, Germany. This enhanced analytical tool
enables novel, sub–angstrom-level resolution TEM techniques, including
scanning probe applications, 3-D reconstruction with tomography, and
in situ observations of specimen responses to stress, temperature, or
chemical environment variations.
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ATOMIC
RESOLUTION: An enhanced TEM system can resolve subangstrom-level
images, such as the silicon transistor gate interface shown here
(inset).
PHOTOS
COURTESY OF FEI |
"The
successful use of an electron beam monochromator to improve the resolution
of a spherical (Cs)-corrected electron microscope marks a major milestone
in the field of electron microscopy," says Michael O'Keefe of the National
Center of Electron Microscopy in Berkeley, CA, who characterized the
breakthrough as an "outstanding achievement.... Theory has long predicted
that a monochromator would be able to push the resolution of the super-twin
lens beyond the 1.4-Å resolution demonstrated with spherical (Cs)-correction
alone. However, the difficulties involved in implementation of a monochromator
without compromising the imaging qualities of the electron beam are
well known."
Also
adding his congratulations was Hannes Lichte of the faculty of mathematics
and natural sciences at the Institute of Structure Physics at Dresden
University (Germany). "For the first time, the authors convincingly
show that in a spherical (Cs)-corrected TEM by additional reduction
of energy spread using a gun monochromator, they extend the total information
limit to significantly better than 0.1 nm....They are not far off the
theoretical limit of about 0.07 nm."